The unknown was insoluble in water and in dilute aqueous base and acid.
1348
The compound is not an acid or base.
Deuterated DMSO and chloroform solvent. Peaks near 6-7 ppm are exchangeable.

ϿvrƤĽϺƾ
¹ͺubϮ|-- `ɺM"f"Ƣ" #

#
Two exchangeable H's mean NH or OH. The 7 other H's are aliphatic and saturated.
#
dummy ms
#
#
#
#
#
Nitrogen was detected.
264048
The compound could be an amine, amide, cyanide, imide etc.
Burnt with a clear flame leaving no residue.
#
The compound is probably saturated.
111 to 113 degrees.
#
The unknown is a solid.
nujol mull
#""""""#""!!!! "!!!!!!!!!!"!!!!""!""##$%%%&'()+,26AHWaq´zslfb^\]afxǹ¾ungULJGC?;=:733321/-,,,++*)***(('&'('''&&'&%%%&&&&&&&()&&%$#####$$$%$"""""""""""####"""#######$%%%&&&&&&((())**+,-./02478:;<>ADGJNSY`fo
ͽxsnigeca_]]]`aaaeghltȿƦ~}zy{ytpnkmqqfa^\YWUQOMIGEFGFKaxoaTOKHIHGC@?><;;<??98754332111110000/0/..//.../137>N[QC;99;@DFGEBA>>?@BCHLRWU[akrutttuv{~wnd`\XRMHEA>:40-*('&$&$&%)*-4Nr[D=;69AFIMWc  
#
The compound is a saturated aliphatic primary amide.
Too high and decomposition occurred.
#
This is typical behaviour of a solid.
Optically inactive.
#
The compound is not chiral.
Not usually measured for a solid.
#
Best to do this measurement on a liquid.
Not usually measured for a solid.
#
Try doing this only with a liquid.
#
#
#
#
#
#
#
dummy cmr
#
#
#
#
#
#
#
#
#
#
#
No precipitate was formed.
2227282950
Unknown 11 is not an aldehyde or ketone.
No positive result.
3344454651
Compounds containing active hydrogen are absent.
Gas evolution (nitrogen) occurred even at low temperature.
#
A primary aliphatic amine or an unsubstituted amide is present
#
#
#
#
#
#
No reaction took place.
14
The unknown is not an ester.
No positive result.
#
Nitro groups are not present in the unknown.
#
#
#
#
#
#
#
#
#
#
#
#
No positive result.
3344454651
The unknown is not an alcohol nor is it a primary or secondary amine.
A distinct colour formed.
#
Unknown 11 is an amide.
No reaction could be seen.
#
The unknown is saturated and not easily oxidised.
#
#
#
No colour change was observed.
232850
The compound is not a sugar.
No apparent change was observed.
#
The unknown does not contain a nitro group.
No reaction was observed.
#
Unknown 11 is not unsaturated nor is it a phenol.
No positive result.
#
THe unknown is not an ether.
No change appeared to take place.
#
Phenolic groups are absent from the unknown.
No colour change was seen.
#
THe unknown is not a primary amine.
#
#
#
No reaction was observed.
#
The unknown is not a primary or secondary amine.
No colour formed.
#
Unknown 22 is not an amino acid.
No nasty smell.
#
The unknown is not a primary amine.
#
#
#
#
#
#
#
#
#
A vigorous reaction occurred.
#
Typical of an oxygen and/or nitrogen containing compound.
#
#
#
No positive result was obtained.
#
The unknown is not a primary amine.
#
#
#
#
#
#
No reaction was visible.
#
No reaction means that the unknown is not a phenol nor is it unsatutrated.
A slow reaction which evolved ammonia on heating with base took place.
#
Unsubstituted amides and also cyanides (nitriles) do this.
No positive result.
3344454651
The unknown is not an alcohol nor is it a primary or secondary amine.
#
#
#
#
#
#
#
#
#
#
#
#
#
#
#
#
#
#
colourless solid
010507
3153
8191
Liquid acid formed which gave a p-bromophenacyl ester with m.p. 60-62 degrees.
Solid with melting range of 183-186 degrees.
2
źɲmb
Ŵrf
solid unsubstituted amide
4
2-methylbutanamide
n-butyramide
ethyl oxamate
methacrylamide
